Autor: Guo, X. - Prolib Integro

Skocz do pozycji: 1.

Tytuł:: Preparation and Characterization of Desensitized ?-HNIW in Solvent-Antisolvent Recrystallizations
Autorzy:: Jiang, X.
Guo, X.
Ren, H.
Jiao, Q.
Tematy:: ε -HNIW
supersaturation
crystal morphology
thermal decomposition
reduced sensitivity; Pokaż więcej
Wydawca:: Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Powiązania:: https://bibliotekanauki.pl/articles/358201.pdf Link otwiera się w nowym oknie
Opis:: The solubility of hexanitrohexaazaisowurtzitane (HNIW) in solvent and solvent-antisolvent mixtures, and the temperature at which the HNIW's polymorph transforms were studied. The solubility of HNIW in solvent-antisolvent mixtures was measured at 30 C and these data were fitted to a generalized solubility curve. Recrystallization experiments were conducted at 30 C in the case of saturation with the volume ratio of ethyl acetate to petroleum ether (chloroform) ranging from 0:1 to 4:1. Desensitized HNIW was obtained by ethyl acetate and petroleum ether crystallization and characterized by Fourier Transform Infrared Spectroscopy (FTIR), X-ray Diffraction (XRD), High Performance Liquid Chromatography (HPLC) and Scanning Electron Microscopy (SEM). The FTIR and XRD spectra confirmed the structural features of ε-HNIW. The blocklike ε-HNIW grains had an average particle size of 160 ?m and high purity (98.52%). The decomposition of ε-HNIW was observed in the temperature range of 225-246 C by Differential Scanning Calorimetry (DSC). Furthermore, the impact and friction sensitivity tests suggested that the desensitized ε-HNIW was less sensitive than raw HNIW. Small scale gap tests with desensitized ε-HNIW showed that these crystals are less sensitive to shock initiation.
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 2.

Tytuł:: Evaluation of Adjustable Thermal Insulations of Tibetan Clothing by Manikin Testing
Ocena możliwości zmian izolacji cieplnej ubiorów tybetańskich przy wykorzystaniu manekina
Autorzy:: Guo, X F
Wang, Y Y
Li, J
Tematy:: Tibetan clothing
style
thermal insulation
clothing area factor
thermal manikin
ubiór tybetański
styl
izolacja cieplna
przewodzenie ciepła
manekin termiczny; Pokaż więcej
Wydawca:: Sieć Badawcza Łukasiewicz - Instytut Biopolimerów i Włókien Chemicznych
Powiązania:: https://bibliotekanauki.pl/articles/232266.pdf Link otwiera się w nowym oknie
Opis:: The thermal insulation of clothing needs to be easily adjusted in an unsteady environment, but this is extremely difficult for most clothing. To reveal the effect of different styles of Tibetan clothing on their thermal property, the total thermal insulations of Tibetan clothing in three typical styles were measured using a thermal manikin. The clothing area factors (fcl) of the Tibetan clothing and body surface area covered by a Tibetan robe were tested with a photographic method. The results showed the following: 1) For similar insulation, fcl of Tibetan clothing is about 0.23 bigger than that of western clothing, estimated from ISO 11079; 2)the style of Tibetan clothing significantly affects the fcl (p < 0.05, fcl = 1.229 + 0.007 BSAC) and the intrinsic thermal insulation (p < 0.05, Icl = 0.166 + 0.016 BSAC); 3)the adjustable thermal insulation of Tibetan clothing proved its adaptability to the large air temperature difference environment on the Tibetan plateau ,which should be valuable for the product development of clothing used in a unsteady environment.
Odzież powinna umożliwiać zmianę jej przewodności cieplnej w niestabilnym środowisku, jednak dla większości odzieży jest to niezwykle trudne. W celu określenia wpływu różnych stylów ubiorów tybetańskich na ich właściwości termiczne określono całkowitą izolację termiczna dla trzech typowych stylów odzieży tybetańskiej przy zastosowaniu manekina termicznego. Wpływ konfiguracji ubioru sprawdzono metodą fotograficzną za pomocą termowizji, określając jednocześnie powierzchniowy współczynnik okrycia ciała fcl. Wykazano, że 1) przy podobnej izolacji fcl ubiorów tybetańskich jest o 0.23 większy od ubiorów zachodnich (ISO11079); 2) styl ubiorów tybetańskich znacząco wpływa na fcl jak i wewnętrzną izolacje cieplną; 3) możliwość regulacji izolacji termicznej tybetańskiego ubioru zapewnia zdolność przystosowania się do dużych różnic temperatury otoczenia na płaskowyżu tybetańskim. Wyniki badań mogą znaleźć zastosowanie w projektowaniu odzieży noszonej w niestabilnym środowisku.
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 3.

Tytuł:: Adsorptive performance of MCM-41 towards hg(II) in water. Adsorption and desorption studies
Autorzy:: Zhai, Q. Z.
Hu, W.-H.
Guo, X.-Y.
Tematy:: electron microscopy
mesoporous silicates
cetyltrimethylammonium bromide
adsorption conditions
mikroskopia elektronowa
krzemiany mezoporowate
bromek cetyltrimethylammonium
warunki adsorpcyjne; Pokaż więcej
Wydawca:: Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Powiązania:: https://bibliotekanauki.pl/articles/208154.pdf Link otwiera się w nowym oknie
Opis:: MCM-41 mesoporous material was prepared under a standard conditions by using cetyltrime-thylammonium bromide as a structure-directing agent and tetraethyl orthosilicate as silica source from the liquid phase at 80 °C. Powder X-ray diffraction and scanning electron microscopy used to characterize the product, showed that the MCM-41material had an average particle size of 110 nm. The synthesized material was used to investigate the effects of acidity, adsorption time, the concentration of Hg²⁺, adsorbent dosage and temperature on the adsorption of Hg²⁺. The results showed that the optimal adsorptive conditions were: pH 5.0, m(MCM-41):mHg²⁺ 6.67, temperature 20 °C and contact adsorption time 60 min, for the initial Hg²⁺concentration of 1.0 mg/cm³. The maximum adsorptive amount of Hg²⁺ was 56.48 mg Hg²⁺/g MCM-41. The results of the desorptive effect of three desorption agents such as HCl, HNO₃ and HAc showed that the best desorbent was HCl at the concentration of 0.10 mol/dm³. The highest desorption efficiency was 77.21% for the desorption time 2 h.
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 4.

Tytuł:: Dynamic-accumulative operation policy of continuous distillation for the purification of anisole
Autorzy:: Wang, Z.
Li, S.
Wang, C.
Guo, X.
Bai, P.
Tematy:: anisole recycling
dynamic-accumulative operation policy
continuous distillation
simulation; Pokaż więcej
Wydawca:: Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Powiązania:: https://bibliotekanauki.pl/articles/779622.pdf Link otwiera się w nowym oknie
Opis:: In the B10 isotope enrichment industry, the purification of anisole mixture makes great sense. A dynamic-accumulative operation policy of continuous distillation (DACD) with repeated filling and dumping of the still is proposed for the separation of trace heavy impurities in the recycled anisole. To simulate and optimize the purification process of anisole, a mathematical model of DACD is derived, and the computer codes are developed in the MATLAB environment. Moreover, the experiment is performed in a pilot-scale distillation column. The results show that the experimental date agrees well with simulation results. DACD could solve the difficulty of flow rate control when the bottom flow rate is very small in continuous distillation. The size of the still in this operation mode is also smaller than that in batch distillation. And the yield of anisole is raised to 99.91%. In a word, DACD is especially suitable for separating trace heavy impurities from the recycled anisole.
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 5.

Tytuł:: Preparation and Properties of Natural Cellulose Fibres from
Otrzymywanie i właściwości folii celulozowych z włókien łykowych
Autorzy:: Qu, L
Tian, M.
Guo, X.
Pan, N
Zhang, X.
Zhu, S
Tematy:: Broussonetia papyrifera (BP)
natural cellulose fibre
fibre extraction
microwave-assisted
włókna celulozowe
włókna łykowe
folia celulozowa
Broussonetia Papyrifera (BP); Pokaż więcej
Wydawca:: Sieć Badawcza Łukasiewicz - Instytut Biopolimerów i Włókien Chemicznych
Powiązania:: https://bibliotekanauki.pl/articles/234492.pdf Link otwiera się w nowym oknie
Opis:: Natural cellulose fibres from Broussonetia papyrifera (L.) Vent. (BP) bast were systematically investigated in this paper. To begin with, BP fibres were successively extracted from BP bast by four different degumming methods, among which the microwave-assisted method exhibited high efficiency. It was found that non-cellulose substances were sufficiently removed or reduced after the degumming process, but the cellulose I structure had not changed from bast to fibres based on the XRD and FTIR results. Meanwhile the BP fibres exhibited high crystallinity (75 ~ 77%), high breaking strength (2.19 ~ 2.39 cN/dtex) and a remarkable moisture region (6.3 ~ 8.7%), but low breaking elongation (1.0 ~ 2.1%). All those results indicated that the BP fibres had properties resembling those of traditional natural cellulose fibres (e.g. cotton and flax); therefore they could be viewed as a promising alternative source for natural cellulose bundle fibres.
Artykuł poświecono systematycznym badaniom naturalnych włókien celulozowych z Broussonetia Papyrifera (BP). Włókna ekstrahowano z włókien łykowych BP poprzez 4 rożne metody odpreparowania pomiędzy z których metoda za pomocą zastosowania ultradźwięków pozwoliła na uzyskanie wysokiej wydajności. Stwierdzono, że nie celulozowe substancje były dostatecznie usunięte lub zredukowane po procesie odpreparowania. Dzięki badaniom XRD i FITR można było wykazać, że struktura celulozy (I) nie zmieniła się pomiędzy włóknami łykowymi i otrzymanymi z nich wyrobami. dalsze badania wykazały źe włókna BP maja wysoką krystaliczność (75 - 77%), wysoką wytrzymałość(2.19 - 2.39 cN/dtex) i znaczną pochłanialność wilgoci (6.3 - 8.7%) natomiast małe wydłużenie przy zerwaniu (1.0 - 2.1%). Wszystkie te wyniki wskazują,że włókna BP posiadają właściwości przypominające właściwości tradycyjnych, naturalnych włókien celulozowych (np. bawełny i lnu). Dlatego też badane włok-na można uważać jako alternatywne źródło naturalnych włókien celulozowych.
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 6.

Tytuł:: Preparation of Twinned Dendrites of Al-Zn Alloy with High Zn Content
Autorzy:: Gao, K.
Song, W.
Fan, L.
Ding, Y.
Guo, X.
Zhang, R.
Tematy:: directional solidification
twinned dendrite
microstructure
growth orientation
deviation angle; Pokaż więcej
Wydawca:: Polska Akademia Nauk. Czytelnia Czasopism PAN
Powiązania:: https://bibliotekanauki.pl/articles/351396.pdf Link otwiera się w nowym oknie
Opis:: Twinned dendrites in Al-Zn alloy with high Zn content (40% wt.%) were successfully prepared by directional solidification. At different directional solidification rates (1000 and 1500 μm/s), microstructures and growth orientation variations of Al twinned dendrite and non-twinned dendrite were characterized. By using the inverted trapezoidal graphite sleeve at 1000 μm/s, Al twinned dendrite were formed to developed feather crystal structures in longitudinal section. Its primary and secondary twinned dendrite were grew along [110] direction. Moreover the deviation angle between [110] direction of Al twinned dendrite and the heat flow direction was about 27.15°. While not using the inverted trapezoidal graphite sleeve at 1000 and 1500 μm/s, Al dendrite was the non-twinned dendrite and the twinned dendrite was not appeared. The experimental results showed that the higher temperature gradient, a certain pulling rate and convection environment were the formation conditions of twinned dendrites.
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 7.

Tytuł:: Palaeo-earthquake events during the late Early Palaeozoic in the central Tarim Basin (NW China): evidence from deep drilling cores
Autorzy:: He, B.
Qiao, X.
Jiao, C.
Xu, Z.
Cai, Z.
Guo, X.
Zhang, Y.
Tematy:: soft-sediment deformation structures
seismites
palaeo-seismicity
Late Ordovician
Silurian
Tazhong 1 Fault
Tarim Basin
struktury deformacji
osady miękkie
sejsmity
ordowik późny
sylur
Kotlina Kaszgarska; Pokaż więcej
Wydawca:: Uniwersytet im. Adama Mickiewicza w Poznaniu
Powiązania:: https://bibliotekanauki.pl/articles/94300.pdf Link otwiera się w nowym oknie
Opis:: Various millimetre-, centimetre- and metre-scale soft-sediment deformation structures (SSDS) have been identified in the Upper Ordovician and Lower-Middle Silurian from deep drilling cores in the Tarim Basin (NW China). These structures include liquefied-sand veins, liquefaction-induced breccias, boudinage-like structures, load and diapir- or flame-like structures, dish and mixed-layer structures, hydroplastic convolutions and seismic unconformities. The deformed layers are intercalated by undeformed layers of varying thicknesses that are petrologically and sedimentologically similar to the deformed layers. The SSDS developed in a shelf environment during the early Late Ordovician and formed initially under shear tensile stress conditions, as indicated by boudinage-like structures; during the latest Ordovician, SSDS formed under a compressional regime. The SSDS in the Lower-Middle Silurian consist mainly of mixed layers and sand veins; they formed in shoreline and tidal-flat settings with liquefaction features indicating an origin under a compressional stress regime. By Silurian times, the centre of tectonic activity had shifted to the south-eastern part of the basin. The SSDS occur at different depths in wells that are close to the syn-sedimentary Tazhong 1 Fault (TZ1F) and associated reversed-thrust secondary faults. Based on their characteristics, the inferred formation mechanism and the spatial association with faults, the SSDS are interpreted as seismites. The Tazhong 1 fault was a seismogenic fault during the later Ordovician, whereas the reversed-direction secondary faults became active in the Early-Middle Silurian. Multiple palaeo-earthquake records reflect pulses and cyclicity, which supports secondary tectonic activity within the main tectonic movement. The range of SSDS structures reflects different developments of tectonic activity with time for the various tectonic units of the centralbasin. The effects of the strong palaeo-earthquake activity coincide with uplift, fault activity and syn-tectonic sedimentation in the study area during the Late Ordovician to Middle Silurian.
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 8.

Tytuł:: Research on the Mechanism and Kinetics of Polymorphic Transitions of ε CL-20 in Composite Systems
Autorzy:: Guo, X.-Y.
Zhang, P.
Xu, J.-J.
Wang, Z.-H.
Jiao, Q.-J.
Tematy:: polymorphic transition
kinetics
activation energy
transition temperature; Pokaż więcej
Wydawca:: Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Powiązania:: https://bibliotekanauki.pl/articles/358032.pdf Link otwiera się w nowym oknie
Opis:: In order to explore the polymorphic transition law for ε-CL-20 in composite systems, the polymorphic transition process of pure ε-CL-20 crystals stimulated by heat was investigated by the X-ray Diffraction (XRD) method, and the kinetic parameters of the polymorphic transition process were calculated (including the apparent activation energy Ea and the pre-exponential factor lnA). Meanwhile the effects of different additives on the polymorphic transition process and kinetics of ε-CL-20 were explored in detail. The experimental results showed that the ε-form tends to transform into the γ- form on heating and that the Ea and lnA for the transition process were 209.97 kJ/mol and 57.47, respectively. The first group of additives clearly promoted the polymorphic transition of ε-CL-20 and lowered the initial transition temperature and the activation energy. The second and third groups of additives inhibited the polymorphic transition of ε-CL-20 and raised the initial transition temperature and the activation energy.
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 9.

Tytuł:: Analysis of the Thermal Behaviour of CL-20, Potassium Perchlorate, Lithium Perchlorate and Their Admixtures by DSC and TG
Autorzy:: Zhang, J.-J.
Guo, X.-J.
Jiao, Q.-J.
Zhang, H.-L.
Li, H.
Tematy:: CL-20
potassium perchlorate
lithium perchlorate
thermal stability
phase transition; Pokaż więcej
Wydawca:: Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Powiązania:: https://bibliotekanauki.pl/articles/358770.pdf Link otwiera się w nowym oknie
Opis:: The thermal decomposition characteristics of CL-20, potassium perchlorate (KP), lithium perchlorate (LP), a CL-20/KP mixture, and a CL-20/LP mixture were studied using thermogravimetry-differential scanning calorimetry (TG-DSC). The DSC curves for KP exhibited three endothermic peaks and one exothermic peak. The first two endothermic peaks correspond to the rhombic-cubic transition and the fusion of KP, respectively, the third indicates the fusion of KCl, while the exothermic peak is attributed to the decomposition of KP. The DSC curves obtained from LP showed four endothermic peaks and one exothermic peak. The first two endothermic peaks indicate the loss of adsorbed water and water of crystallization, while the third and fourth are associated with the fusion of LP and LiCl, respectively; the exothermic peak is due to the decomposition of LP. The presence of KP had little effect on the thermal decomposition of CL-20 while the addition of LP increased the temperature at which CL-20 exhibits an exothermic peak. In addition, the thermal decomposition of LP appeared to be catalyzed by the presence of CL-20.
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 10.

Tytuł:: Direct synthesis of dimethyl carbonate and propylene glycol using potassium bicarbonate as catalyst in supercritical CO₂
Autorzy:: Wen, Y.
Zhang, R.
Cang, Y.
Zhang, J.
Liu, L.
Guo, X.
Fan, B.
Tematy:: direct synthesis
dimethyl carbonate
carbon dioxide
potassium bicarbonate
supercritical fluids; Pokaż więcej
Wydawca:: Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Powiązania:: https://bibliotekanauki.pl/articles/778066.pdf Link otwiera się w nowym oknie
Opis:: The improved one-pot synthesis of dimethyl carbonate and propylene glycol from propylene oxide, supercritical carbon dioxide, and methanol with potassium bicarbonate as the catalyst has been reported in this paper. As far as we know, it is the first time to use potassium bicarbonate only as the catalyst in the production process which is simple and cheap. Satisfactory conversion rate of propylene oxide and yield of the products could be achieved at the optimized conditions with quite a small amount of by-products. Our new method offers an attractive choice for the production of dimethyl carbonate in large-scale industry efficiently and environmental friendly.
Dostawca treści:: Biblioteka Nauki

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