- Tytuł:
- Assay of the Insensitive High Explosive FOX-7 by Non-Aqueous Titration
- Autorzy:
-
Nandi, A. K.
Paramasivan, P.
Singh, S. K.
Mandal, A. K.
Pandey, R. K. - Tematy:
-
1,1-diamino-2,2-dinitroethene
FOX-7
non-aqueous titration
N,N-dimethylformamide - Pokaż więcej
- Wydawca:
- Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
- Powiązania:
- https://bibliotekanauki.pl/articles/358156.pdf Link otwiera się w nowym oknie
- Opis:
- A non-aqueous titration method was developed to assay the insensitive high explosive 1,1-diamino-2, 2-dinitroethene (FOX-7). The weak acidic nature of FOX-7 (pKa 10.6) was exploited in the assay method. The sample was dissolved in the protophilic solvent N, N-dimethylformamide and titrated against sodium methoxide solution in benzene/methanol using azo violet as indicator. FOX-7 samples obtained from regular batch operations were assayed by this method and the results were compared with that of a recrystallized sample. The method is simple, rapid and has good accuracy and precision.
- Dostawca treści:
- Biblioteka Nauki
Artykuł