Temat: Green synthesis - Prolib Integro

Skocz do pozycji: 1.

Tytuł:: Chitosan-based nanocomposites modified with reduced graphene oxide prepared via green synthesis
Autorzy:: Kosowska, K.
Domalik-Pyzik, P.
Jagiełło, J.
Lipińska, L.
Chłopek, J.
Tematy:: nanocomposites
graphene oxide
green synthesis; Pokaż więcej
Wydawca:: Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Powiązania:: https://bibliotekanauki.pl/articles/284680.pdf Link otwiera się w nowym oknie
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 2.

Tytuł:: Green chemistry for the preparation of silver nanoparticles using mint leaf leaves extracts and evaluation of their antimicrobial potential
Autorzy:: Aziz, Wisam J.
Jassim, Haneen A.
Tematy:: Green synthesis
Mentha (Mint)
Silver Nanoparticles; Pokaż więcej
Wydawca:: Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Powiązania:: https://bibliotekanauki.pl/articles/1112556.pdf Link otwiera się w nowym oknie
Opis:: The aim of this study was to develop a green synthesis of silver nanoparticles using mint plant leaves extracts. The fresh suspension of plant extracts was yellowish-green in color. However, after the addition of AgNO3 within 15min, the suspension showed a change in color to dark brown after 5 hours of incubation at room temperature. The formation of silver nanoparticles was confirmed using UV-Vis spectral analysis and revealed silver surface plasmon resonance band to be in a range around 200-500 nm. The XRD pattern showed the characteristic bragg peaks of (111), (200) and (220) planes of the face center cubic (FCC) silver nanoparticles AgNPS. Under scanning electron microscope (SEM), silver nanoparticles with a mean particle size of 26 nm and a spherical shape were most frequently observed. In testing, the synthesized AgNPs colloidal solution showed better antibacterial activity against both Gram-positive and Gram-negative bacterial strains. The diameter of the inhibition zones of AgNPs at 50 µg/ml concentration against bacterial strains such as Bacillus subtilis and Escherichia coli were 25 mm and 20 mm, respectively.
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 3.

Tytuł:: Easy, Simplistic and Green Synthesis of Various Benzimidazole and Benzoxazole Derivatives Using PEG400 as a Green Solvent
Autorzy:: Khunt, M. D.
Kotadiya, V. C.
Viradiya, D. J.
Baria, B. H.
Bhoya, U. C.
Tematy:: PEG-400
Benzimidazole
Benzoxazole
Green synthesis; Pokaż więcej
Wydawca:: Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Powiązania:: https://bibliotekanauki.pl/articles/411999.pdf Link otwiera się w nowym oknie
Opis:: An improved environmentally benign procedure for the synthesis of various benzimidazole and benzoxazole derivatives using green solvent PEG400. We have optimized the reaction condition and it was found that PEG400 was believed to be best as compared to PEG200, PEG600 and PEG800 at 80 to 85 °C. This method provides a novel route for the synthesis of benzimidazole and benzoxazole derivatives. The main attractive features of this process are a mild reaction conditions, easy workup procedure and good to excellent yield. The structures of all the synthesized compounds were confirmed by 1H NMR, IR, MASS and Elemental Analysis.
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 4.

Tytuł:: Comparison of conventional and green approaches to the synthesis of aromatic Schiff bases
Autorzy:: Kołodziej, Beata
Tematy:: sustainable development
Schiff bases
green chemistry
green synthesis; Pokaż więcej
Wydawca:: Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Powiązania:: https://bibliotekanauki.pl/articles/59124236.pdf Link otwiera się w nowym oknie
Opis:: The chemical industry is one of the key elements in improving the quality of human life. At the same time, it generates pollution influencing the ecosystem and our health. To limit or remove some of the reasons of pollution for two decades less harmful approaches to the synthesis of various organic compounds were developed. Among organic compounds, azomethines, also known as Schiff bases, are of particular interest in biochemistry, medicine, and pharmacy. For over twenty years many novel approaches to the synthesis of these compounds have been investigated. Toxic solvents (benzene, toluene) have been replaced with water, fruit juice, or white egg, and in many cases, temperature and time of process were significantly reduced. In the review, conventional and green approaches to the synthesis of Schiff bases are presented with a focus on the effectiveness of these methods, including advantages and disadvantages.
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 5.

Tytuł:: Ball milling preparation of spent graphite supported zero-valent iron-copper to degrade tetracycline in water
Autorzy:: Hang, Xingping
Wu, Xiaotian
Song, Wei
Chen, Shuai
Tematy:: sustainable development
Schiff bases
green chemistry
green synthesis; Pokaż więcej
Wydawca:: Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Powiązania:: https://bibliotekanauki.pl/articles/59124257.pdf Link otwiera się w nowym oknie
Opis:: In this study, graphite and copper from spent LIBs were used to prepare graphite supported zero-valent iron-copper (ZVI-Cu/G) by ball milling, to improve the reactivity of ZVI. The structure, composition, morphology, and properties of ZVI-Cu/G were fully analyzed. The removal performances of tetracycline by ZVI-Cu/G were tested under different reaction conditions. Graphite and copper improve the dispersion, specific surface area and reactivity of the material. Operational factors, material dosage of 1 g/L, initial pH of 3, temperature of 25 °C, and H2O2 concentration of 2 mM, contribute to the best tetracycline removal rate, being 100% in 30 min for 30 mg/L tetracycline solution. The reaction data fits a pseudo first-order model. Tetracycline removal rate was as high as 90% even in the 3rd round of reuse. This study reports a novel ZVI material with high tetracycline removal rate.
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 6.

Tytuł:: Bio synthesis and characterization of silver nanoparticles using Lagenaria siceraria leaf extract and their antibacterial activity
Autorzy:: Anandh, B.
Muthuvel, A.
Emayavaramban, M.
Tematy:: green synthesis
silver nanoparticles
Lagenaria siceraria
antibacteriala activity; Pokaż więcej
Wydawca:: Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Powiązania:: https://bibliotekanauki.pl/articles/412277.pdf Link otwiera się w nowym oknie
Opis:: The present investigation demonstrates the formation of silver nanoparticles by the reduction of the aqueous silver metal ions during exposure to the Lagenaria siceraria leaf extract. The synthesized AgNPs have characterized by UV-visible spectroscopy, X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FT-IR) techniques. AgNPs formation has screened by UV-visible spectroscopy through colour conversion due to surface plasma resonance band at 427 nm. X-ray diffraction (XRD) confirmed that the resulting AgNPs are highly crystalline and the structure is face centered cubic (fcc). FT-IR spectrum indicates the presence of different functional groups present in the biomolecules capping the nanoparticles. Further, inhibitory activity of AgNPs and leaf extract were tested against human pathogens like gram-pastive (Staphylococcus aureus, Bacillus subtilis), gram-negative (Escherichia coli and Pseudomonas aeruginosa). The results indicated that the AgNPs showed moderate inhibitory actions against human pathogens than Lagenaria siceraria leaf extract, demonstrating its antimicrobial value against pathogenic diseases.
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 7.

Tytuł:: Synthesis of silver nanoparticles by aqueous extract of Zingiber officinale and their antibacterial activities against selected species
Autorzy:: Hussain, Zawar
Jahangeer, Muhammad
ur Rahman, Shafiq
Ihsan, Tamanna
Sarwar, Abid
Ullah, Najeeb
Aziz, Tariq
Alharbi, Metab
Alshammari, Abdulrahman
Alasmari, Abdullah F.
Tematy:: Nanotechnology
Antibacterial activity
Silver-nanoparticles
green synthesis
Ginger; Pokaż więcej
Wydawca:: Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Powiązania:: https://bibliotekanauki.pl/articles/27315653.pdf Link otwiera się w nowym oknie
Opis:: Silver nanoparticles have special plasmonic and antibacterial characteristics that make them efficient in a variety of commercial medical applications. According to recent research, chemically synthesized silver nanoparticles are harmful even in low concentrations. It was crucial to identify appropriate synthesis methods that may have low costs and be nontoxic to the environment. Zingiber officinale (ginger) extracts used to prepare silver nanoparticles were inexpensive and environmentally friendly, and the best physicochemical characteristics were analyzed. Silver nanoparticles were characterized by using UV-visible spectroscopy, Scanning electron microscopy (SEM), and X-ray diffraction (XRD). The surface Plasmon resonance peak at 425 nm was observed using UV-Visible spectroscopy. Scanning electron microscopy observed that the nanoparticles were spherical and ranged in size from 5 to 35 nm. The XRD pattern values of 2θ: 38.2° , 46.3° , and 64.58° are used to determine the planes (111), (200), and (220). The silver nanoparticle’s existence was verified by the face-centered cubic (FCC). Silver nanoparticles were found to have antibacterial efficacy against gram-positive Staphylococcus and gram-negative bacteria such as Pseudomonas aeruginosa, Klebsiella Aerogenes, Salmonella, Staphylococcus and Escherichia coli. The antibacterial activity of silver nanoparticles was observed using the agar well diffusion (AWD) method at three different concentrations (100 μg/ ml, 75 μg/ml, and 50 μg/ml). The zone of inhibition measured against the bacterial strains pseudomonas Aeruginosa, Klebsiella aerogenes, Escherichia coli, Salmonella and Staphylococcus which were (18.4±1.25 mm, 16.9±0.74 mm, 14.8±1.25 mm), (16.8±0.96 mm, 14.6±0.76 mm, 14.0±1.15 mm), (19.7±0.76 mm, 18.2±0.66 mm, 15.4±1.15 mm), (16.6±0.67 mm, 14.2±0.23 mm, 12.8±0.78 mm) and (12±0.68 mm, 10±0.20 mm, 08±0.15 mm). These nanoparticles’ potent antibacterial properties may enable them to be employed as nanomedicines for a variety of gramnegative bacterial illness treatments.
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 8.

Tytuł:: Green synthesis of cobalt–zinc ferrites and their activity in dye elimination via adsorption and catalytic wet peroxide oxidation
Autorzy:: Liaskovska, Mariia
Tatarchuk, Tetiana
Kotsyubynsky, Volodymyr
Opis:: Zinc-substituted cobalt ferrites were obtained by a green method using a black grape extract as a reductant and fuel. XRD analysis confirmed the spinel structure of the synthesized ferrites. An increase in the lattice constant is explained by increased Zn content. SEM analysis confirmed changes in surface morphology, whereas FTIR spectra demonstrated the presence of organic species in the samples, which originated from grape extract. The content of Co(II) ions in octahedral sites as a function of the ratio between Fe(III) ions in A- and B-sites was calculated from Mössbauer data. $pH_{PZC}$ rose from 7.85 to 8.13 with an increase in zinc content, indicating a positive charge of the adsorbent surface at natural pH. The adsorption–catalytic properties of the spinel samples were investigated in terms of Congo Red (CR) dye removal. The mechanism of CR adsorption on the ferrite surface includes electrostatic and donor–acceptor interactions with the adsorbent surface. Furthermore, the sample with x(Zn) = 0.4 exhibited the highest degradation rate constant $k = 0.102 min^{−1}$ in the peroxide oxidation of CR, whereas the sample with x(Zn) = 1.0 exhibited the highest adsorption capacity. The electron transfer between ferrite samples and hydrogen peroxide was evidenced using electrochemical tests. The green-synthesized Co-Zn ferrites demonstrate a big potential as adsorbents/catalysts for water treatment.
Dostawca treści:: Repozytorium Uniwersytetu Jagiellońskiego

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Skocz do pozycji: 9.

Tytuł:: PEG mediated eco-friendly one pot sunthesis of benzylamine coumarin derivatives using multicomponent reactant
Autorzy:: Viradiya, D. J.
Kotadiya, V. C
Khunt, M. D.
Baria, B. H.
Bhoya, U. C.
Tematy:: one pot reaction
benzylamine coumarin derivative
green synthesis
PEG-400; Pokaż więcej
Wydawca:: Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Powiązania:: https://bibliotekanauki.pl/articles/412545.pdf Link otwiera się w nowym oknie
Opis:: A green resourceful, eco-friendly and facile protocol was developed for the synthesis of benzylamine coumarin derivatives by the reaction of 4-hydroxy coumarin, secondary amine and aromatic aldehyde in the presence of PEG400 as a solvent as well as catalyst at room temperature. A wide range of functional groups were tolerated in the developed protocol. The structures of all the synthesized compounds were confirmed by 1H NMR, IR, MASS and Elemental Analysis. The target molecules were obtained in good to excellent yield applying this method.
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 10.

Tytuł:: Soymida febrifuga aqueous root extract maneuvered silver nanoparticles as mercury nanosensor and potential microbicide
Autorzy:: Sowmyya, T.
Lakshmi, G. Vijaya
Tematy:: Characterization
Green synthesis
Mercury nanosensor
Microbicide
Silver nanoparticles
Soymida febrifuga; Pokaż więcej
Wydawca:: Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Powiązania:: https://bibliotekanauki.pl/articles/1158479.pdf Link otwiera się w nowym oknie
Opis:: The present communication reports a rapid, uncomplicated, sustainable and facile method of eco-friendly synthesis of silver nanoparticles (AgNPs). The pressing need for the development of benign, profitable and eco-friendly alternative routes has inspired researchers to explore plant extracts as safer replacements to hazardous chemicals. In the present study, a benign method of synthesis of AgNPs using Soymida febrifuga aqueous root extract has been developed. The characterization studies of synthesized AgNPs revealed spherical morphology and crystalline nature of AgNPs. The average particle size was 21.81 nm. The synthesized AgNPs were employed as mercury nanosensor for the selective and sensitive detection of toxic mercury ions in water and soil samples. The AgNPs showed a marked visual color change and change in surface plasmon resonance band on interaction with mercury ions. The greater selectivity of AgNPs towards mercury ions was observed. The limit of detection of mercury by 100 μL of colloidal AgNPs was found to be 2×10-4 M visually and 1.332×10-5 M spectrophotometrically in water samples and ×-4 M visually and 22.3×10-5 M spectrophotometrically in soil samples. The method makes use of a small quantity of AgNPs for detection of mercury in water and soil samples. The method proposed in the present study provides a rapid, selective and sensitive method for detection of mercury ions in environmental water and soil samples. The synthesized AgNPs were also used as effective microbicidal agents. The microbicidal potential of the synthesized AgNPs was checked against two gram positive and gram negative bacterial strains.
Dostawca treści:: Biblioteka Nauki

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