Temat: TEM characterization

Skocz do pozycji: 1.

Tytuł:: The Wear Mechanisms Description Of Multilayer Coatings, Performed By Transmission Electron Microscopy – An Overview Of The Own Research Work
Opis mechanizmu zużycia wielowarstwowych powłok w oparciu o transmisyjną mikroskopię elektronową – przegląd własnych badań doświadczalnych
Autorzy:: Major, Ł.
Tematy:: multilayer coatings
TEM characterization
wear mechanisms
powłoki wielowarstwowe
TEM
mechanizm zużycia; Pokaż więcej
Wydawca:: Polska Akademia Nauk. Czytelnia Czasopism PAN
Powiązania:: https://bibliotekanauki.pl/articles/351356.pdf Link otwiera się w nowym oknie
Opis:: The aim of the presented paper was to describe the wear mechanisms operating at the small length scale in multilayer coatings subjected to a mechanical testing. A hybrid PLD system (Pulsed Laser Deposition connected with magnetron sputtering) was used for the multi-layer coating deposition. Coatings were subjected to indentation, ball-on disc wear and scratch adhesion tests. Microstructure of the as-deposited coating and after mechanical tests was studied using the Scanning (SEM) and the Transmission (TEM) Electron Microscopes. The research work revealed that application of innovative multilayer coatings may allow to predict their life time and to steer their properties.
Celem pracy było określenie mechanizmów zużycia wielowarstwowych powłok tribologicznych, poddanych testom mechanicznym na zużycie. Powłoki wytwarzane przy zastosowaniu hybrydowego układu PLD (technika laserowej ablacji połączona z rozpylaniem magnetronowym) poddane zostały mechanicznym testom na zużycie (indentacja oraz test kula-tarcza), a także testowi przylegania powłoki do podłoża (test zarysowania). Charakterystykę mikrostruktury powłok przed i po testach mechanicznych przeprowadzono za pomocą skaningowej (SEM) oraz transmisyjnej (TEM) mikroskopii elektronowej. Badania wykazały, że poprzez stosowanie innowacyjnych powłok wielowarstwowych można przewidzieć czas ich eksploatacji oraz dają możliwość sterowania właściwościami.
Dostawca treści:: Biblioteka Nauki

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Tytuł:: A Novel Identification Method of Thermal Resistances of Thermoelectric Modules Combining Electrical Characterization Under Constant Temperature and Heat Flow Conditions
Autorzy:: Siouane, S.
Jovanović, S.
Poure, P.
Tematy:: Thermoelectric Module (TEM)
thermal resistance
contact thermal resistance
electrical characterization
identification
electrical models; Pokaż więcej
Wydawca:: EEEIC International Barbara Leonowicz Szabłowska
Powiązania:: https://bibliotekanauki.pl/articles/136156.pdf Link otwiera się w nowym oknie
Opis:: The efficiency of a Thermoelectric Module (TEM) is not only influenced by the material properties, but also by the heat losses due to the internal and contact thermal resistances. In the literature, the material properties are mostly discussed, mainly to increase the well-known thermoelectric figure of merit ZT. Nevertheless, when a TEM is considered, the separate characterization of the materials of the p and n elements is not enough to have a suitable TEM electrical model and evaluate more precisely its efficiency. Only a few recent papers deal with thermal resistances and their influence on the TEM efficiency; mostly, the minimization of these resistances is recommended, without giving a way to determine their values. The aim of the present paper is to identify the internal and contact thermal resistances of a TEM by electrical characterization. Depending on the applications, the TEM can be used either under constant temperature gradient or constant heat flow conditions. The proposed identification approach is based on the theoretical electrical modeling of the TEM, in both conditions. It is simple to implement, because it is based only on open circuit test conditions. A single electrical measurement under both conditions (constant-temperature and constant-heat) is needed. Based on the theoretical electrical models, one can identify the internal and thermal resistances.
Dostawca treści:: Biblioteka Nauki

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Skocz do pozycji: 3.

Tytuł:: Microstructure characterization of localized corrosion wear of Cr/Cr2N+ a-C:H/a-C:H:Cr multilayer coatings on carbon fiber composites
Autorzy:: Janusz, M.
Major, L.
Lackner, J. M.
Grysakowski, B.
Krawiec, H.
Tematy:: nano-composite multilayer coatings
micro-corrosion
carbon fiber composite
microstructure characterization
TEM
charakterystyka mikrostruktury
nanokompozyty wielowarstwowe
kompozyt z włóknami węglowymi; Pokaż więcej
Wydawca:: Polska Akademia Nauk. Czytelnia Czasopism PAN
Powiązania:: https://bibliotekanauki.pl/articles/200247.pdf Link otwiera się w nowym oknie
Opis:: The use of carbon fiber composites (CFC) for different applications is widespread. Carbon-based materials show, however, significant oxidative degradation in air. Modern materials are subjected to aggressive, corrosive environment. This type of environment may strongly reduce their mechanical properties. For the protection of CFC, it was necessary to apply coatings to the composite surface. In the presented paper, a chromium/chromium nitride (Cr/Cr2N) multilayer structure has been selected as the inner part. The outer part of the coating was a hydrogenated amorphous carbon (a-C:H), gradually implanted by Cr nanocrystals. The application of transmission electron microscopy (TEM) indicated that the proposed deposition method allowed the formation of a Cr/Cr2N multilayer of Λ = 150 nm, topped with a-C:H+ Cr23C6 composite of a varied carbides density. The micro-hardness of the deposited coatings was up to 14 GPa (at a load of 2 and 5 mN). The microstructure of the deposited coatings was described in detail by means of TEM in the authors’ recently published paper [1]. This paper is a continuation thereof, aimed at describing microstructure changes after a localized corrosion process. In order to study localized corrosion in coatings, particularly in metallic (Cr) interlayers, the potential measurements and voltammetry experiments were performed in a Ringer solution. The open-circuit potential reaches stable values after a sufficient time period. The results indicated that the presence of a-C:H+Cr23C6, the outer part of the coating, speeds up the localized corrosion process in Cr interlayers in the inner part of a coating.
Dostawca treści:: Biblioteka Nauki

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