Temat: phase analysis - Prolib Integro

Skocz do pozycji: 1.

Tytuł:: Phase Analysis of Different Liquid Ratio on Metakaolin/Dolomite Geopolymer
Autorzy:: Syauqi Sauffi, Ahmad
Wan Mastura, Wan Ibrahim
Mohd Mustafa Al Bakri, Abdullah
Ibrahim, Masdiyana
Ahmad, Romisuhani
Ahmad Zaidi, Fakhryna
Tematy:: geopolymer
metakaolin
dolomite
phase analysis; Pokaż więcej
Wydawca:: Polska Akademia Nauk. Czytelnia Czasopism PAN
Powiązania:: https://bibliotekanauki.pl/articles/2048822.pdf Link otwiera się w nowym oknie
Opis:: Geopolymer is widely studied nowadays in various scope of studies. Some of the ongoing studies are the study of the various materials towards the geopolymer strength produced. Meanwhile, some of the studies focus on the mixing of the geopolymer itself. This paper discussed the phase analysis of metakaolin/dolomite geopolymer for different solid to the liquid ratio which was, 0.4, 0.6, 0.8, and 1.0, and the properties that affected the geopolymer based on the phases. The constant parameters in this study were the percentage of metakaolin and dolomite used. The metakaolin used was 80% meanwhile dolomite usage was 20%. Besides that, the molarity of NaOH used is 10M and the alkaline activator ratio used is 2.0. All the samples were tested at 28 days of curing. The results show that the 0.8 solid to the liquid ratio used gave better properties compare to other solid to liquid ratio. The phases analyzed were quartz, sillimanite, mullite, and faujasite. The 0.8 S/L ratio shows the better properties compared to others by the test of phase analysis, compressive strength morphology analysis, and functional group analysis.
Dostawca treści:: Biblioteka Nauki

Artykuł

na półce

Skocz do pozycji: 2.

Tytuł:: Influence of die forging parameters on the microstructure and phase composition of Inconel 718 alloy
Wpływ warunków kucia matrycowego na mikrostrukturę oraz skład fazowy stopu Inconel 718
Autorzy:: Bunsch, A.
Kowalska, J.
Witkowska, M.
Tematy:: Inconel 718
microstructure
texture
phase analysis
recrystallization; Pokaż więcej
Wydawca:: Polska Akademia Nauk. Czytelnia Czasopism PAN
Powiązania:: https://bibliotekanauki.pl/articles/355862.pdf Link otwiera się w nowym oknie
Opis:: The object of the present investigation was Inconel 718 alloy. The material in the initial state and after forging at the temperatures of 1100°C and 1000°C was examined. Diffraction analyses indicate that a nickel-based γ solid solution is a dominating phase in the alloy (so-called nickel austenite). Apart from a solid solution, which constitutes the matrix, certain volume fractions of the other phase were detected e.g. δ phase and carbides. It was found that, due to thermo-mechanical-treatment at both temperatures, the phase composition of Inconel 718 was considerably changed in comparison to the initial state. On the contrary, differences in the temperature of forging did not significantly influence the alloy constitution. However, both of the temperatures of forging result in distinct texture intensity. Microstructure observations indicate that forging at 1000C° led to recrystallization by creation of the new recrystallizated grains near or on the grain boundaries of existing deformed grains. After forging at 1100°C, the microstructure was fully recrystallized at the whole volume of the material.
W pracy przedstawiono wyniki badan wykonanych na stopie niklu Inconel 718. Przebadano materiał w stanie wyjściowym i po kuciu w temperaturach 1100 i 1000°C. Wykonane badania dyfrakcyjne wskazują, ze faza dominującą w stopie jest faza γ roztwór Fe w Ni, często nazywany austenitem niklowym. Oprócz tej fazy, w stopie występują takie fazy jak δ oraz węgliki. Proces kucia w porównaniu do stanu wyjściowego wpływa na skład fazowy (następuje rozpuszczenie niektórych faz i być może przesycenie osnowy), natomiast różnica w temperaturze przeróbki plastycznej nie wpłynęła znacząco na skład fazowy. Obserwacje mikrostruktury wskazują, ze kucie w temperaturze 1100°C prowadzi do pełnej rekrystalizacji dynamicznej, zaś w temperaturze 1000°C rekrystalizacja zachodzi tylko poprzez tworzenie nowych ziarn na granicach ziarn lub w obszarach przy granicach istniejących odkształconych ziarn. Równocześnie, obserwuje się różnice w stopniu steksturowania materiału.
Dostawca treści:: Biblioteka Nauki

Artykuł

na półce

Skocz do pozycji: 3.

Tytuł:: Application of X-Ray Diffraction to Analyse Phase Composition of Aluminium Alloys for Plastic Working
Autorzy:: Pachut, K.
Żelechowski, J.
Boczkal, S.
Tematy:: aluminium alloys
X-ray diffraction
qualitative phase analysis; Pokaż więcej
Wydawca:: Polska Akademia Nauk. Czytelnia Czasopism PAN
Powiązania:: https://bibliotekanauki.pl/articles/354144.pdf Link otwiera się w nowym oknie
Opis:: An attempt was made to determine phase composition of commercial aluminium alloys using X-ray diffraction. Samples for phase composition analysis were selected from the group of aluminium alloys covered by the EN 573-3:2013 standard [1]. Representative samples were taken from eight groups of alloys with different chemical composition (at least one sample from each group). The diffraction intensity was measured with a standard X-ray diffractometer in Bragg-Brentano geometry in a way that allowed identification of the weakest diffraction peaks. As a results of the performed research it has been shown that X-ray phase analysis can be used to identify the matrix of aluminium alloys, Si and crystalline intermetallic phases such as Mg₂Si, Al_93.38Cu_6.02Fe₂₄Si_16.27, Al_4.01MnSi_0.74, MgZn₂, Al₁₇ (Fe_3.2Mn_0.8)Si₂, Al₆₅Cu₂₀Fe₁₅, and Cu₃Mn₂Al. The detectability limit of the above-mentioned phases is better than 0.5%. The research has also shown that X-ray phase analysis is applicable in the investigation of phase transformations taking place in aluminium alloys.
Dostawca treści:: Biblioteka Nauki

Artykuł

na półce

Skocz do pozycji: 4.

Tytuł:: Microstructure of Archaeological 17th Century Cast Copper Alloys
Autorzy:: Konieczny, J.
Labisz, K.
Głowik-Łazarczyk, K.
Ćwiek, J.
Wierzbicki, Ł.
Tematy:: metallography
archaeometallurgy
microstructure
excavations
phase analysis
metalografia
archaeometalurgia
mikrostruktura
wykopaliska; Pokaż więcej
Wydawca:: Polska Akademia Nauk. Czytelnia Czasopism PAN
Powiązania:: https://bibliotekanauki.pl/articles/382152.pdf Link otwiera się w nowym oknie
Opis:: In Poland, researchers have a very strong interest in archaeometallurgy, which, as presented in classical works, focuses on dating artefacts from the prehistoric and early medieval periods in the form of cast iron and copper castings. This study, extending the current knowledge, presents the results of a microstructure investigation into the findings from the Modern era dating back to the late Middle Ages. The investigated material was an object in the form of a heavy solid copper block weighing several kilograms that was excavated by a team of Polish archaeologists working under the direction of Ms Iwona Młodkowska-Przepiórowska during works on the marketplace in the city of Czestochowa during the summer of 2009. Pre-dating of the material indicates the period of the seventeenth century AD. The solid copper block was delivered in the form of a part shaped like a bell, named later in this work as a “kettlebell”. To determine the microstructure, the structural components, chemical composition, and homogeneity, as well as additives and impurities, investigations were carried out using light microscopy, scanning electron microscopy including analysis of the chemical composition performed in micro-areas, and qualitative X-ray phase analysis in order to investigate the phase composition. Interpretation of the analytical results of the material’s microstructure will also help modify and/or develop new methodological assumptions to investigate further archaeometallurgical exhibits, throwing new light on and expanding the area of knowledge of the use and processing of seventeenth-century metallic materials.
Dostawca treści:: Biblioteka Nauki

Artykuł

na półce

Skocz do pozycji: 5.

Tytuł:: Influence of High-Temperature Oxidizing Conditions on AlCoCrCuNi High Entropy Alloys with and without Silicon Addition
Autorzy:: Gawel, R.
Rogal, Ł.
Przybylski, K.
Matsuda, Kenji
Tematy:: high entropy alloy
high temperature oxidation
phase analysis
alloying element; Pokaż więcej
Wydawca:: Polska Akademia Nauk. Czytelnia Czasopism PAN
Powiązania:: https://bibliotekanauki.pl/articles/2106569.pdf Link otwiera się w nowym oknie
Opis:: Initial investigations on oxidation behaviour and phase transformations of equimolar AlCoCrCuNi high entropy alloy with and without 1 at.% silicon addition during 24-hr exposure to air atmosphere at 1273 K was carried out in this work. After determining the oxidation kinetics of the samples by means of thermogravimetric analysis, the morphology, chemical and phase compositions of the oxidized alloys were determined by means of scanning electron microscopy, energy dispersive X-ray spectroscopy and X-ray diffraction analysis. Additional cross-section studies were performed using transmission electron microscopy combined with energy dispersive X-ray spectroscopy and selected area electron diffraction. From all these investigations, it can be concluded that minor silicon addition improves the oxidation kinetics and hinders the formation of an additional FCC structure near the surface of the material.
Dostawca treści:: Biblioteka Nauki

Artykuł

na półce

Skocz do pozycji: 6.

Tytuł:: Phase Composition of Urban Soils by X-Ray Diffraction and Mössbauer Spectroscopy Analysis
Autorzy:: Kierlik, P.
Hanc-Kuczkowska, A.
Męczyński, R.
Matuła, I.
Dercz, G.
Tematy:: Mössbauer spectroscopy
X-ray diffraction
environmental protection
qualitative phase analysis
topsoil; Pokaż więcej
Wydawca:: Polska Akademia Nauk. Czytelnia Czasopism PAN
Powiązania:: https://bibliotekanauki.pl/articles/353120.pdf Link otwiera się w nowym oknie
Opis:: The main purpose of this study was to identify the mineral composition of soil sample taken from the upper layer of topsoil. High absorption of chemical substance is a characteristic for humus-organic layer of topsoil. The source of those substance could be a pollutant emitted to the atmosphere by human activity. The research area includes Upper Silesia region, which is the most industrial region of Poland. In the present study, the phase composition of the top soil separates were analyzed by using X-raydiffraction and Mössbauer spectroscopy. X-ray diffraction analysis revealed the presence of seven mineral phases in the material magnetic separated by lower current (quartz, illite, kaolinite, Fe³⁺ oxides, hematite, magnetite and pyrite). In case of higher current were identified four phases (quartz, muscovite, kaolinite and K_0.94 Na_0.06 (AlSi₃ O₈ )). Mössbauer spectroscopy was used for an extensive analysis of iron-containing phases (pyrrhotite, magnetite, aluminosilicate oxides with Fe³⁺ and kaolinite/Fe²⁺ silicate).
Dostawca treści:: Biblioteka Nauki

Artykuł

na półce

Skocz do pozycji: 7.

Tytuł:: Reaction Kinetics and Morphological Study of TiNb2O7 Synthesized by Solid-State Reaction
Autorzy:: Choi, S. H.
Ali, B.
Choi, K. S.
Hyun, S. K.
Sim, J. J.
Choi, W. J.
Joo, W.
Lim, J. H.
Lee, T. H.
Kim, T. S.
Park, K. T.
Tematy:: solid state reaction
kinetic analysis
quantitative phase analysis
TiNb2O7 synthesis; Pokaż więcej
Wydawca:: Polska Akademia Nauk. Czytelnia Czasopism PAN
Powiązania:: https://bibliotekanauki.pl/articles/355326.pdf Link otwiera się w nowym oknie
Opis:: Although TiNb₂O₇ is regarded as a material with high application potential in lithium-ion batteries (LIBs) and solid-oxide fuel cells (SOFCs), it has been difficult to find suitable cost-effective conditions for synthesizing it on a commercial scale. In this study, TiNb₂O₇ compounds were synthesized by a solid state synthesis process. For stoichiometrically precise synthesis of the TiNb₂O₇ phase, the starting materials, TiO₂ and Nb₂O₅ were taken in a 1:1 molar ratio. Activation energy and reaction kinetics of the system were investigated at various synthesis temperatures (800,1000,1200, and 1400°C) and for various holding durations (1,5,10, and 20 h). Furthermore, change in the product morphology and particle size distribution were also evaluated as a function of synthesis temperature and duration. Additionally, quantitative phase analysis was conducted using the Rietveld refinement method. It was found that increases in the synthesis temperature and holding time lead to increase in the mean particle size from 1 to 4.5 μm. The reaction rate constant for the synthesis reaction was also calculated.
Dostawca treści:: Biblioteka Nauki

Artykuł

na półce

Skocz do pozycji: 8.

Tytuł:: Metallurgical analysis of the causes of failure of the hardening furnace conveyor belt
Autorzy:: Merda, A.
Klimaszewska, K.
Sroka, M.
Golański, G.
Tematy:: microstructure
X-ray phase analysis
precipitates
failure
mikrostruktura
rentgenowska analiza fazowa
osady
niepowodzenie; Pokaż więcej
Wydawca:: Stowarzyszenie Komputerowej Nauki o Materiałach i Inżynierii Powierzchni w Gliwicach
Powiązania:: https://bibliotekanauki.pl/articles/378641.pdf Link otwiera się w nowym oknie
Opis:: Purpose: The aim of the tests was to analyze the microstructure and mechanical properties of a section of the hardening furnace conveyor belt serviced at the temperature of 880-920°C in the carburizing atmosphere, in the context of determining the probable causes of its failure. Design/methodology/approach: The scope of performed tests included: chemical composition analysis of the steel and particles, microstructure investigated using optical and scanning electron microscopy, X-ray phase analysis. Findings: The analysis of the chemical composition showed that the examined material was austenitic steel X15CrNiSi25-21 (S310). Performed metallurgical tests showed that after the service the examined steel was characterized by austenitic structure with numerous precipitates of diverse morphology. In the structure the sigma phase particles and probably the M23C6 carbides precipitates were observed. The continuous grid of precipitates on the boundaries of grains (mainly the sigma phase) and the influence of the cyclic changing heat loads (or thermo-mechanical loads) were the main causes of failure of the analysed detail. Research limitations/implications: The aim of the work was to determine the probable causes of damage of the material used for a conveyor belt of a hardening furnace. Practical implications: The results of investigation and analysis of the metallographic of het-resisting austenitic steel X15CrNiSi25-21 (S310) after service at the temperature of 880-920°C are presented. Originality/value: The paper presents the results of research on the microstructure and mechanical properties of the section of hardening furnace conveyor belt made of creepresisting austenitic steel. The aim of the performed tests was to determine the probable causes of damage of the analysed detail.
Dostawca treści:: Biblioteka Nauki

Artykuł

na półce

Skocz do pozycji: 9.

Tytuł:: Iron-containing phases in metallurgical and coke dusts as well as in bog iron ore
Autorzy:: Szumiata, T.
Rachwał, M.
Magiera, T.
Brzózka, K.
Gzik-Szumiata, M.
Gawroński, M.
Górka, B.
Kyzioł-Komosińska, J.
Tematy:: metallurgical dusts
coke dusts
bog ore
phase analysis
Mössbauer spectrometry
magnetic susceptibility; Pokaż więcej
Wydawca:: Instytut Chemii i Techniki Jądrowej
Powiązania:: https://bibliotekanauki.pl/articles/148303.pdf Link otwiera się w nowym oknie
Opis:: Several samples of dusts from steel and coke plants (collected mostly with electro filters) were subjected to the investigation of content of mineral phases in their particles. Additionally, sample of bog iron ore and metallurgical slurry was studied. Next, the magnetic susceptibility of all the samples was determined, and investigations of iron-containing phases were performed using transmission Mössbauer spectrometry. The values of mass-specific magnetic susceptibility varied in a wide range: from 59 to above 7000 × 10−8 m3kg−1. The low values are determined for bog iron ore, metallurgical slurry, and coke dusts. The extremely high was obtained for metallurgical dusts. The Mössbauer spectra and X-ray diffraction patterns point to the presence of the following phases containing iron: hematite and oxidized magnetite (in coke and metallurgical dusts as well as metallurgical slurry), traces of magnetite fi ne grains fraction (in metallurgical dusts), amorphous glassy silicates with paramagnetic Fe3+ and Fe2+ ions, traces of pyrrhotite (in coke dusts), α-Fe and nonstoichiometric wüstite (in metallurgical slurry), as well as ferrihydrite nanoparticles (in bog iron ore). For individual samples of metallurgical dusts, the relative contributions of Fe2+/3+ ions in octahedral B sites and Fe2+ ions in tetrahedral A sites in magnetite spinel structure differs considerably.
Dostawca treści:: Biblioteka Nauki

Artykuł

na półce

Skocz do pozycji: 10.

Tytuł:: Phase space analysis of semiconductor laser dynamics
Autorzy:: Grześ, Paweł
Michalska, Maria
Świderski, Jacek
Tematy:: semiconductor laser
laser dynamics
phase space analysis
rate equations; Pokaż więcej
Wydawca:: Polska Akademia Nauk. Stowarzyszenie Elektryków Polskich
Powiązania:: https://bibliotekanauki.pl/articles/59112935.pdf Link otwiera się w nowym oknie
Opis:: The dynamics of semiconductor lasers are modelled in the time domain using a pair of differential equations known as rate equations. The analysis, based on temporal solutions of these equations, yields practical results utilised in various applications. Alternatively, an analysis employing the phase space method, a well-established analytical tool in applied mathematics, provides a more comprehensive perspective on semiconductor laser dynamics. The main purpose of this paper is to provide a detailed and intuitive introduction to phase space analysis in the context of semiconductor laser dynamics. The goal is to offer an easily comprehensible description of the mentioned method, placing emphasis on the graphical representation and physical interpretation of the results. The method effectiveness is shown through its application to selected practical problems. Furthermore, semiconductor laser dynamics can be treated as an illustrative example, showcasing the applicability of the method, which can be readily extended to other types of lasers or even more advanced dynamic systems.
Dostawca treści:: Biblioteka Nauki

Artykuł

na półce

Informacja

Wyszukujesz frazę "phase analysis" wg kryterium: Temat